Structural Properties of Hydrothermally-Synthesized Cu2O/Cu Nanocomposites for Gas Sensing Applications

Document Type : Research Paper

Authors

1 The General Directorate of Education in the Province of Baghdad/Rusafa-2, Ministry of Education, Baghdad, IRAQ

2 Open Educational College, Baghdad, IRAQ

Abstract

A simple hydrothermal synthesis method with CuSO4 of copper was used to prepare Cu2O/Cu nanoparticles. Samples were characterized by X-ray- diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). With an increase in reaction time and a temperature increase. In the end, the following products were obtained: Cu2O octahedron microcrystals, Cu2O/Cu composite particles, and a wide range of nanowires. A study of the gas sensitivity of the samples (products) towards NO2 gas was carried out. Through the results, it appeared that the sensors prepared for the compound Cu2O/Cu at a temperature of 65°C and for 20 min showed a very good gas sensitivity (optimal). The very good gas sensitivity indicated that the Cu2O/Cu compounds may have very wide applications as gas sensors.A simple hydrothermal synthesis method with CuSO4 of copper was used to prepare Cu2O/Cu nanoparticles. Samples were characterized by X-ray- diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). With an increase in reaction time and a temperature increase. In the end, the following products were obtained: Cu2O octahedron microcrystals, Cu2O/Cu composite particles, and a wide range of nanowires. A study of the gas sensitivity of the samples (products) towards NO2 gas was carried out. Through the results, it appeared that the sensors prepared for the compound Cu2O/Cu at a temperature of 65°C and for 20 min showed a very good gas sensitivity (optimal). The very good gas sensitivity indicated that the Cu2O/Cu compounds may have very wide applications as gas sensors.

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